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T h e anomaly was r e m o v e d when Lewis et al. (1960) showed that the complexes were hydrides, for example: H R h C l ( A s M e P h ) 2 . In other words, the true oxidation state of the metal 2 2 in these complexes is + 3 . Departures of m o m e n t s from the spin-only values predicted for particu­ lar oxidation states m a y occur for reasons other than the existence of an orbital contribution. , 1962). Pauling predicted that diamagnetic complexes of nickel(II) w o u l d be square-coordinated—a configuration that had not been observed for nickel 26 D .

J. Inorg. & Nuclear Chem. 17, 186. Arrhenus, S. (1887). Z. physik. Chem. (Leipzig) 1, 631. Chem. Soc. p. 586. Barclay, G. , and Hoskins, B. F. (1962). Barclayi, G. , and Nyholm, R . S. (1953). Chem. & Ind. (London) p . 378. , and Pearson, R . G. (1958). " Wiley, New York. , and Sillen, L. G. (1957). " Chem. Soc. (London) Spec. Publ. No. 7. Blau, F. (1898). Monatsh. 19, 647. Blomstrand, C. W . (1869). " Heidelberg. Brintzinger, H . , and Muller, U. (1943). Z. anorg. u. allgem. Chem. 251, 285. , and Fornara (1904).

1939). Alexander, W . , and Pauson, P. L. (1961). J. Inorg. & Nuclear Chem. 17, 186. Arrhenus, S. (1887). Z. physik. Chem. (Leipzig) 1, 631. Chem. Soc. p. 586. Barclay, G. , and Hoskins, B. F. (1962). Barclayi, G. , and Nyholm, R . S. (1953). Chem. & Ind. (London) p . 378. , and Pearson, R . G. (1958). " Wiley, New York. , and Sillen, L. G. (1957). " Chem. Soc. (London) Spec. Publ. No. 7. Blau, F. (1898). Monatsh. 19, 647. Blomstrand, C. W . (1869). " Heidelberg. Brintzinger, H . , and Muller, U.

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